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Novel 4-ferrocenyl-8-(phenylthio)-1,2,3,4-tetrahydroquinoline: Design, synthesis and spectral characterization
dc.contributor.author | Minić, Aleksandra | |
dc.contributor.author | Bugarinović, Jovana | |
dc.contributor.author | Pešić, Marko | |
dc.contributor.author | Ilić Komatina, Danijela | |
dc.date.accessioned | 2022-09-26T10:09:39Z | |
dc.date.available | 2022-09-26T10:09:39Z | |
dc.date.issued | 2019 | |
dc.identifier.uri | https://platon.pr.ac.rs/handle/123456789/665 | |
dc.description.abstract | Herein, we report design, synthesis and spectral characterization of novel 4-ferrocenyl-8-(phenylthio)-1,2,3,4-tetrahydroquinoline. Desired synthesis was achieved in three reaction steps, with a good overall yield (67%). First step included aza-Michael addition of 2-(phenylthio)aniline to 1-ferrocenylpropenone, subsequently, the obtained ketone was smoothly reduced to the corresponding 1,3-amino alcohol. The final step was an intramolecular cyclization prompted by acetic acid, proceeding via corresponding α-ferrocenyl carbocation. The synthesized compounds have been isolated pure, and their structure have been undoubtedly confirmed by standard spectral techniques (1H NMR, 13C NMR, IR and elemental analyses). | en_US |
dc.language.iso | en_US | en_US |
dc.publisher | The University Thought - Publication in Natural Sciences | en_US |
dc.rights | Ауторство-Некомерцијално-Без прерада 3.0 САД | * |
dc.rights.uri | http://creativecommons.org/licenses/by-nc-nd/3.0/us/ | * |
dc.title | Novel 4-ferrocenyl-8-(phenylthio)-1,2,3,4-tetrahydroquinoline: Design, synthesis and spectral characterization | en_US |
dc.title.alternative | The University Thought - Publication in Natural Sciences | en_US |
dc.type | clanak-u-casopisu | en_US |
dc.description.version | publishedVersion | en_US |
dc.identifier.doi | 10.5937/univtho9-20839 | |
dc.citation.volume | 9 | |
dc.subject.keywords | Tetrahydroquinoline ring | en_US |
dc.subject.keywords | Ferrocenes | en_US |
dc.subject.keywords | Intramolecular cyclization | en_US |
dc.type.mCategory | M52 | en_US |
dc.type.mCategory | openAccess | en_US |
dc.type.mCategory | M52 | en_US |
dc.type.mCategory | openAccess | en_US |